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The present invention relates to a method for fabricating cylindrical fine particles and in particular to a method for fabricating fine particles of a spherical shape having a controlled particle size distribution.
Generally, finely divided powders obtained by the wet process are used as catalyst raw materials, and many hydrophobic catalysts, fine catalyst particles and catalyst carrier materials used for polymerization and mass transfer in the process of a living catalyst polymerization have been proposed. As for the catalyst carrier materials, they are roughly classified into inorganic and organic carrier materials.
Of these carrier materials, organic carrier materials such as silica, alumina and zeolite have strong hydrophobicity and a large surface area and are thus excellent in such properties as water resistance and adsorption ability. In particular, zeolite has excellent adsorption ability and can remove an object to be adsorbed from the catalyst particle by adsorption, allowing the catalyst particles to become adsorbent. It also has a high hydrophobicity. It is thus noted that the zeolite carrier material is a promising catalyst carrier material.
Conventional methods for producing zeolite particles are classified in such a manner that basic raw materials are crystallized to grow zeolite and such a crystallized zeolite is aggregated by ion exchange. Typical of such methods is a method in which a reaction system is crystallized by the addition of an alkali metal salt as a crystal nucleation agent. Particularly, zeolite particles obtained by the sodium ion exchange crystallization are stable and have a low particle size distribution.
On the other hand, a finely divided powder having a controlled particle size distribution, such as a spherically shaped powder having small particles dispersed on the periphery has conventionally been obtained by spraying water droplets or water jet through a discharge nozzle to produce drops or particles of an approximately spherical shape having a particle size distribution. For example, JP-A No. 55-111201 discloses a method in which a suspension consisting of a certain type of zeolite particles with a high ratio of spherical particles and water is discharged through a spray head to produce fine particles of a spherical shape having a particle size distribution. However,
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